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Excerpt of the 2D HSQC-NOESY NMR of 9mer-I-F showing the expected intra-residue NOEs and the key NOE (GlcF-6/GlcC-2) between the two strands of the hairpin (288 K, mixing time 300 ms, D2O, 800 MHz). The asterisks indicate signals belonging to an impurity (Supplementary Figs. 67 and 68).
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