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19F ssNMR spectra collected on as-synthesized LMTOF1244-800, -900, -1000 (using Li6MnO4, MnF2, and TiO2precursors) and the reference sample synthesized using conventional precursors of LiF, Li2O, MnO, and TiO2at 1000 °C. A long recycle delay of 20 s was used to ensure full relaxation of all the19FssNMR signals between scans for quantification. The spectra were scaled according to the sample mass in the rotor and the number of scans used during the data acquisition.

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