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Superimposed 1 H/ 1 H COSY and 1 H/ 1 H NOESY NMR spectra show cross-peaks between protons of Rha I-1 with β Thr-8 and of Rha II-1 with Rha I-3 (red dashed lines), confirming the nature of the two bonds (Source data https://doi.org/10.5281/zenodo.14918824 ).
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