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The signal intensities of reactant and product in hyperpolarized 1H NMR spectra over the time course of the spectral acquisition. Each data point took 2 s to acquire and each is recorded immediately after the previous data point. Time t= 0 corresponds to the starting point of spectral acquisition, which is ca 5–10 s after addition of CF3SO2OCH3. Note that each signal is normalized to its intensity in the first spectrum.
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